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Synthesis and Lithiation Mechanisms of Dirutile and Rutile

XRD confirmed no dirutile-to-rutile phase transitions to occur after the two hour milling cycle with carbon. A two-phase sample of diru-tile and rutile LiMnF 4 was obtained by milling dirutile LiMnF 4 for 12hours at 500 rpm with carbon. All milling was performed under inert atmostphere by assembling and reopening ball mill jars in an argon